Skip to main navigation menu Skip to main content Skip to site footer

Research Articles

Vol. 13 No. sp1 (2026): Recent Advances in Agriculture

Process optimization of spray drying conditions for custard apple (Annona squamosa L.) pulp powder using response surface methodology

DOI
https://doi.org/10.14719/pst.12008
Submitted
26 September 2025
Published
18-02-2026

Abstract

Response Surface Methodology (RSM) was employed to optimize the spray-drying conditions for the production of custard apple (Annona squamosa L.) pulp powder using maltodextrin as a carrier agent. The pulp of the custard apple is highly perishable and contains numerous bioactive compounds that are heat sensitive. This complicates the production of a stable powder that retains its nutrients during conventional drying methods. The inlet and outlet air temperatures were identified as the most significant process factors affecting the physicochemical, nutritional and functional properties of the produced powder. Higher inlet temperature enhanced drying efficiency and augmented powder output; however, they also accelerated the degradation of ascorbic acid and exacerbated non-enzymatic browning. Higher outlet temperatures positively influenced functional attributes such as wettability, swelling capacity and water absorption capability. The developed RSM models exhibited a high degree of predictive accuracy (R² > 0.92), with experimental and anticipated values closely aligned, indicating their adequacy. Multi-response optimization identified the optimal drying conditions, with an inlet temperature of 175.2 °C and an outlet temperature of 90 °C. The custard apple powder exhibited low residual moisture, moderate hygroscopicity, substantial vitamin C retention, negligible browning and favorable immediate properties that facilitated reconstitution. The results indicate that optimal spray-drying conditions can produce high quality custard apple powder, suitable for use as a functional ingredient in ready-to-drink beverages, nutraceuticals and fortified foods.

References

  1. 1. Kalidindi N, Thimmaiah NV, Jagadeesh NV, Nandeep R, Swetha S, Kalidindi B. Antifungal and antioxidant activities of organic and aqueous extracts of Annona squamosa Linn. leaves. J Food Drug Anal. 2015;23:795-802. https://doi.org/10.1016/j.jfda.2015.04.012
  2. 2. Shrivastava A, Tripathi AD, Paul V, Rai DC. Optimization of spray drying parameters for custard apple (Annona squamosa L.) pulp powder development using response surface methodology with improved physicochemical attributes and phytonutrients. LWT. 2021;151:112091. https://doi.org/10.1016/j.lwt.2021.112091
  3. 3. Souza M, Mesquita A, Souza P, Borges G, Silva T, Converti A, et al. New functional non-dairy mixed tropical fruit juice microencapsulated by spray drying: physicochemical characterization, bioaccessibility, genetic identification and stability. LWT. 2021;152:112271. https://doi.org/10.1016/j.lwt.2021.112271
  4. 4. Shishir MRI, Chen W. Trends of spray drying: a critical review on drying of fruit and vegetable juices. Trends Food Sci Technol. 2017;65:49-67. https://doi.org/10.1016/j.tifs.2017.05.006
  5. 5. Tonon RV, Brabet C, Hubinger MD. Influence of drying air temperature and carrier agent concentration on the physicochemical properties of acai juice powder. Food Sci Technol. 2009;29:444-50. https://doi.org/10.1590/S0101-20612009000200034
  6. 6. Patil V, Chauhan AK, Singh RP. Optimization of the spray-drying process for developing guava powder using response surface methodology. Powder Technol. 2014;253:230-36. https://doi.org/10.1016/j.powtec.2013.11.033
  7. 7. Shishir MR, Taip FS, Aziz NA, Talib RA, Hossain Sarker MS. Optimization of spray drying parameters for pink guava powder using response surface methodology. Food Sci Biotechnol. 2016;25(2):461-68. https://doi.org/10.1007/s10068-016-0064-0
  8. 8. Sin CL. Production and properties of shelf-stable spray-dried powder from enzyme-treated soursop (Annona muricata L.) fruit PhD [dissertation]. Malaysia: Universiti Putra Malaysia; 2017.
  9. 9. Reji M, Kumar R. Response surface methodology: an overview to analyze multivariate data. Indian J Microbiol Res. 2022;9:241-8. https://doi.org/10.18231/j.ijmr.2022.042
  10. 10. Cai YZ, Corke H. Production and properties of spray-dried Amaranthus betacyanin pigments. J Food Sci. 2000;65(7):1248-52. https://doi.org/10.1111/j.1365-2621.2000.tb10273.x
  11. 11. Kumar PS, Keran DA, Pushpavalli S, Shiva KN, Uma S. Effect of cellulose and gum derivatives on physicochemical, microstructural and prebiotic properties of foam-mat dried red banana powder. Int J Biol Macromol. 2022;218:44-56. https://doi.org/10.1016/j.ijbiomac.2022.07.071
  12. 12. Hasan F, Nazir A, Sobti B, Tariq H, Karim R, Al-Marzouqi AH, et al. Dehydration of date fruit (Phoenix dactylifera L.) for the production of natural sweet powder. NFS J. 2022;27:13-20. https://doi.org/10.1016/j.nfs.2022.02.002
  13. 13. Association of Official Analytical Chemists. Official methods of analysis. 18th ed. Gaithersburg (MD); 2006
  14. 14. Li D, Chen R, Liu J, Liu C, Deng L, Chen J. Characterizing and alleviating the browning of Choerospondias axillaris fruit cake during drying. Food Control. 2022;132:108522. https://doi.org/10.1016/j.foodcont.2021.108522
  15. 15. Quek SY, Chok NK, Swedlund P. The physicochemical properties of spray-dried watermelon powders. Chem Eng Process. 2007;46(5):386-92. https://doi.org/10.1016/j.cep.2006.06.020
  16. 16. Phosanam A, Chandrapala J, Zisu B, Adhikari B. Storage stability of powdered dairy ingredients: a review. Dry Technol. 2021;39(11):1529-53. https://doi.org/10.1080/07373937.2021.1910955
  17. 17. Jaya S, Das H. Effect of maltodextrin, glycerol monostearate and tricalcium phosphate on vacuum dried mango powder properties. J Food Eng. 2004;63(2):125-34. https://doi.org/10.1016/S0260-8774(03)00135-3
  18. 18. Mauer LJ, Forny L, Meunier VD, Taylor LS. Optimizing the quality of food powder products: the challenges of moisture-mediated phase transformations. Annu Rev Food Sci Technol. 2019;10(1):457-78. https://doi.org/10.1146/annurev-food-032818-121224
  19. 19. Wang A, Zhong Q. Drying of probiotics to enhance the viability during preparation, storage, food application and digestion: a review. Compr Rev Food Sci Food Saf. 2024;23(1):13287. https://doi.org/10.1111/1541-4337.13287
  20. 20. Sharma R, Nath PC, Seth D. Optimization of spray-drying conditions using response surface methodology, physicochemical characterization and shelf-life estimation of pineapple powder. Sustain Food Technol. 2023;1(5):750-61. https://doi.org/10.1039/D3FB00008G
  21. 21. Nguyen M. Effects of spray drying conditions on the physicochemical and antioxidant properties of the Gac (Momordica cochinchinensis) fruit aril powder. J Food Eng.; 2022.
  22. 22. Cruz-Padilla J, Reyes V, Cavender G, Chotiko A, Gratzek J, Mis Solval K. Comparative analysis of concurrent, mixed flow and combined spray drying configurations on the physicochemical characteristics of Satsuma mandarin (Citrus unshiu) juice powders. Foods. 2023;12(18):3514. https://doi.org/10.3390/foods12183514
  23. 23. Kha TC, Nguyen CT, Tran LT, Truong TT. Effects of pretreatment and air drying temperature on noni fruit powder. Food Sci Biotechnol. 2021;30(12):1519-26. https://doi.org/10.1007/s10068-021-00982-0
  24. 24. Miao S, Roos YH. Isothermal study of nonenzymatic browning kinetics in spray-dried and freeze-dried systems at different relative vapor pressure environments. Innov Food Sci Emerg Technol. 2006;7(3):182-94. https://doi.org/10.1016/j.ifset.2005.11.001
  25. 25. Chng GY, Chang LS, Pui LP. Effects of maltodextrin concentration and inlet temperature on the physicochemical properties of spray-dried kuini powder. Asia Pac J Mol Biol Biotechnol. 2020;28:113-31. https://doi.org/10.35118/apjmbb.2020.028.4.10
  26. 26. Henao-González D, David D, Torres-Oquendo J, Amaral Sobral PJ, Vega-Castro O. Design and optimization of a strawberry-based dispersion to produce a spray drying functional powdered product fortified with folic acid and zinc. Food Bioprod Process. 2024;147:105-14. https://doi.org/10.1016/j.fbp.2024.05.017
  27. 27. Patil V, Chauhan AK. Optimization of the spray-drying process for developing guava powder using response surface methodology. Powder Technol. 2014;253:230-36. https://doi.org/10.1016/j.powtec.2013.11.033
  28. 28. Suo K, Yang Z, Wu L, Zhang Y, Feng Y, Xu B, et al. Enhancing drying characteristics and quality of fruits and vegetables using biochemical drying improvers: a comprehensive review. Compr Rev Food Sci Food Saf. 2025;24(1):e70094. https://doi.org/10.1111/1541-4337.70094
  29. 29. Oliveira SM, Brandao TR, Silva CL. Influence of drying processes and pretreatments on nutritional and bioactive characteristics of dried vegetables: a review. Food Eng Rev. 2016;8(2):134-63. https://doi.org/10.1007/s12393-015-9124-0
  30. 30. Shrivastava A, Tripathi AD, Paul V, Rai DC. Optimization of spray drying parameters for custard apple (Annona squamosa L.) pulp powder development using response surface methodology with improved physicochemical attributes and phytonutrients. LWT. 2021;151:112091. https://doi.org/10.1016/j.lwt.2021.112091

Downloads

Download data is not yet available.